Batch autoclaves consist of a pressure vessel equipped with various components like a stirring mechanism, heating system, and sensors for temperature and pressure. The typical process involves:
1. Loading: Adding reactants and catalyst into the autoclave. 2. Sealing: Ensuring the system is airtight. 3. Heating and Pressurizing: Bringing the system to the desired temperature and pressure. 4. Reaction: Allowing the reaction to proceed for a specified duration. 5. Cooling and Depressurizing: Bringing the system back to ambient conditions. 6. Unloading: Collecting the products for analysis.
