sample integrity

How to Ensure Sample Integrity?

To ensure sample integrity, researchers should adhere to best practices at each stage of sample handling:
Sample Preparation
During sample preparation, it is essential to use clean and appropriate equipment to avoid contamination. The sample should be prepared in an environment with controlled temperature and humidity to prevent any unwanted reactions.
Sample Storage
Samples should be stored in controlled environments that match the stability requirements of the substances involved. Proper labeling and documentation are also crucial to avoid mix-ups and ensure traceability.
Sample Handling
When handling samples, researchers should use appropriate techniques to minimize exposure to air, moisture, or any other reactive substances. Using inert atmospheres, such as nitrogen or argon, can help in maintaining the integrity of sensitive samples.
Analytical Techniques
Choosing the right analytical techniques is vital for maintaining sample integrity. Techniques like X-ray diffraction (XRD), nuclear magnetic resonance (NMR), and Fourier transform infrared spectroscopy (FTIR) should be employed and calibrated correctly to ensure accurate characterization of the sample.

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